ÏÖ´úũҵÉú²úÖÐũҩµÄÆÕ±éÓ¦Ó㬣¬£¬£¬£¬£¬£¬£¬ÒѾ³ÉΪ¿ÕÆøÎÛȾµÄÖ÷ҪȪԴ֮һ¡£¡£¡£¡£¡£ÅçÈ÷ºóµÄũҩ¿ÉÒÔÂþÑÜÓÚ¿ÕÆø¡¢Ë®ºÍÍÁÈÀÖУ¬£¬£¬£¬£¬£¬£¬£¬¶øÖ±½ÓÊ©ÓÃÓÚÅ©×÷ÎïµÄũҩÔò»á»Ó·¢µ½¿ÕÆøÖС£¡£¡£¡£¡£ÓлúÂÈũҩ×÷ΪÌìÏÂÉÏÉú²úºÍʹÓõÄũҩ֮һ£¬£¬£¬£¬£¬£¬£¬£¬Õý¾ÓÉÖÖÖÖ;¾¶ÎÛȾ¿ÕÆø¡£¡£¡£¡£¡£ÎªÁ˸üºÃµÄ¼ì²â¿ÕÆøÖкÛÁ¿ÓлúÂÈũҩ£¬£¬£¬£¬£¬£¬£¬£¬Ê¹ÓÃÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒǾßÓмì³öÏ޵ͣ¬£¬£¬£¬£¬£¬£¬£¬¶¨ÐÔÄÜÁ¦Ç¿¡¢¶¨Á¿×¼È·µÈÌØµã£¬£¬£¬£¬£¬£¬£¬£¬ÒÑÆÕ±éÓ¦ÓÃÓÚ¿ÕÆøÖкÛÁ¿Å©Ò©²ÐÁôµÄ¼ì²â¡£¡£¡£¡£¡£
luck18¹ÙÍøÒÇÆ÷Ò»Ö±ÖÂÁ¦ÓÚΪ¿Í»§Ìṩ¸üÍêÉÆµÄ½â¾ö¼Æ»®£¬£¬£¬£¬£¬£¬£¬£¬ÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇGC-MS 6800¿ÉÓÃÓÚÇéÐÎ¿ÕÆøÖÐÓлúÂÈũҩµÄ¼ì²â¡£¡£¡£¡£¡£
1.ÒÇÆ÷¼ò½é
GC-MS 6800ÊÇluck18¹ÙÍøÒÇÆ÷È«ÐÄ´òÔìµÄÒ»¿î¸ßÐÔ¼Û±ÈÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇ£¬£¬£¬£¬£¬£¬£¬£¬¾ßÓÐÍêÈ«µÄ×ÔÖ÷֪ʶ²úȨ£¬£¬£¬£¬£¬£¬£¬£¬ÓµÓжàÏîÊÖÒÕ£¬£¬£¬£¬£¬£¬£¬£¬¿ÉÆÕ±éÓ¦ÓÃÓÚÇéÐα£»£»£»£»£»¤¡¢µç×ÓµçÆ÷¡¢Ò½Ò©¡¢Ê¯ÓÍ»¯¹¤¡¢Ê³ÎïÇå¾²¡¢·Ä֯Ƥ¸ïµÈ¶àÐÐÒµÖÐÓк¦ÎïÖʵļì²â¡£¡£¡£¡£¡£
ͼ1. GC-MS 6800ÆøÏàÉ«Æ×-ÖÊÆ×ÁªÓÃÒÇÍâ¹Ûͼ
2 ʵÑ鲿·Ö
2.1 ²âÊÔÔÀí
ÓôóÁ÷Á¿²ÉÑùÆ÷½«ÇéÐÎ¿ÕÆøÆøÏàºÍ¿ÅÁ£ÎïÖеÄÓлúÂÈÊÕÂÞµ½ÂËĤºÍ¾Û°±õ¥ÅÝÄ£¨PUF£©ÉÏ£¬£¬£¬£¬£¬£¬£¬£¬ÓÃÒÒÃÑ-Õý¼ºÍé»ìÏýÈܼÁÌáÈ¡£¡£¡£¡£¡£¬£¬£¬£¬£¬£¬£¬£¬ÌáȡҺ¾Å¨Ëõ¡¢¾»»¯ºó£¬£¬£¬£¬£¬£¬£¬£¬ÆøÏàÉ«Æ×ÊèÉ¢£¬£¬£¬£¬£¬£¬£¬£¬ÖÊÆ×ÒǼì²â£¬£¬£¬£¬£¬£¬£¬£¬Æ¾Ö¤±£´æÊ±¼äºÍÌØÕ÷Àë×ÓÆ·Ã²±È¶¨ÐÔ£¬£¬£¬£¬£¬£¬£¬£¬Äڱ귨¶¨Á¿¡£¡£¡£¡£¡£
2.2 Ö÷ÒªÒÇÆ÷×°±¸¡¢ºÄ²ÄºÍÊÔ¼Á
GC-MS 6800 ÆøÏàÉ«Æ×-ÖÊÆ×ÁªÓÃÒÇ£¨luck18¹ÙÍø£©
´óÁ÷Á¿²ÉÑùÆ÷£¨600/AFPUF1001K Òâ´óÀû£©
Ë÷ʽÌáÈ¡ÒÇ£¨É½¶«º£ÄÜ£©
µª´µÒÇ£¨±±¾©ÓÅêÉÍÅ½á¿Æ¼¼ÓÐÏÞ¹«Ë¾£©
¹ÌÏàÝÍȡװÖã¨À³²®Ì©¿Æ£©
±ûͪ£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©
Õý¼ºÍ飨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©
ÒÒÃÑ£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©
¶þÂȼ×Í飨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©
ÎÞË®ÁòËáÄÆ£ºÆÊÎö´¿£¨½ËÕǿʢ¹¦Ð§»¯Ñ§ÓÐÏÞ¹«Ë¾£©
ÂÈ»¯ÄÆ£ºÆÊÎö´¿£¨½ËÕǿʢ¹¦Ð§»¯Ñ§ÓÐÏÞ¹«Ë¾£©
ÁòË᣺ÃܶÈ1.84g/cm3£¬£¬£¬£¬£¬£¬£¬£¬Óż¶´¿£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©
ÂÈ»¯ÄÆÈÜÒº£º50g/L£¬£¬£¬£¬£¬£¬£¬£¬ÏÖÓÃÏÖÅä
ÄÚ±êʹÓÃÒº£ºÝì-d10,10ug/ml£¬£¬£¬£¬£¬£¬£¬£¬Õý¼ºÍéÉèÖã¨Öйú±ê×¼ÎïÖÊ£©
Ìæ»»ÎïʹÓÃÒº£ºÆp-d12£¬£¬£¬£¬£¬£¬£¬£¬2ug/ml£¨Öйú±ê×¼ÎïÖÊ£©
±ê×¼´¢±¸Òº£º10mg/L,ÈܼÁÕý¼ºÍ飨Öйú±ê×¼ÎïÖÊ£©
µªÆø£º´¿¶È¡Ý99.999%£¨¿ÕÆø»¯¹¤£©
º¤Æø£º´¿¶È¡Ý99.999%£¨¿ÕÆø»¯¹¤£©
2.3ÒÇÆ÷²âÊÔÌõ¼þ
É«Æ×Öù£ºDB-5MS£¬£¬£¬£¬£¬£¬£¬£¬30m¡Á0.25mm¡Á0.25¦Ìm£¨Agilent£©
ÖùÏä³ÌÐòÉýÎÂÌõ¼þ£º80¡æ£¨1min£©20¡æ/min 200¡æ 5¡æ/min 280¡æ£¨5min£©
½øÑù¿Úζȣº280¡æ£»£»£»£»£»ÆøÖʽӿÚζȣº280¡æ£»£»£»£»£»Àë×ÓԴζȣº280¡æ
ÔØÆø£ºº¤Æø£¬£¬£¬£¬£¬£¬£¬£¬´¿¶È¡Ý99.999%£¬£¬£¬£¬£¬£¬£¬£¬Á÷ËÙ1.0mL/min
µçÀë·½·¨£ºEI£»£»£»£»£»µçÀëÄÜÁ¿£º70eV
½øÑù·½·¨£º²»·ÖÁ÷½øÑù£¬£¬£¬£¬£¬£¬£¬£¬·ÖÁ÷±È20£º1£»£»£»£»£»½øÑùÁ¿£º1.0¦ÌL
²â¶¨·½·¨£ºTIC£¨FULL SCAN£©¶¨ÐÔ£¨É¨Ãè¹æÄ££º45-450amu£©£¬£¬£¬£¬£¬£¬£¬£¬SIMģʽ¶¨Á¿¡£¡£¡£¡£¡£

ͼ2. ÓлúÂÈũҩ»¯ºÏÎï×ÜÀë×ÓÁ÷É«Æ×ͼ
1¡ª¦Á-ÁùÁùÁù£»£»£»£»£»2¡ª¦Â-ÁùÁùÁù£»£»£»£»£»3¡ª¦Ã -ÁùÁùÁù£»£»£»£»£»4¡ªÝì-D10£¨Äڱ꣩£»£»£»£»£»5¡ª¦Ä-ÁùÁùÁù£»£»£»£»£»6¡ªÆßÂÈ£»£»£»£»£»7¡ª°¬ÊϼÁ£»£»£»£»£»8¡ª»·ÑõÆßÂÈ B£»£»£»£»£»9¡ª¦Ã-Âȵ¤£»£»£»£»£»£»£»£»£»£»10¡ªÁòµ¤ I£»£»£»£»£»11¡ª¦Á-Âȵ¤£»£»£»£»£»12¡ª4,4'-DDE£»£»£»£»£»13¡ªµÒÊϼÁ£»£»£»£»£» 14¡ªÒìµÒÊϼÁ£»£»£»£»£»15¡ªÁòµ¤ II£»£»£»£»£»16¡ª4,4'- DDD£»£»£»£»£» 17¡ªÒìµÒÊÏÈ©£»£»£»£»£»18¡ªÁòµ¤ÁòËáõ¥£»£»£»£»£»19¡ª 4,4'-DDT£»£»£»£»£»20¡ªÒìµÒÊÏͪ£»£»£»£»£» 21¡ª¼×Ñõ DDT£»£»£»£»£»22¡ªÆp-D12£¨²ÉÑùÌæ»»Î
3 С½á
½ÓÄÉ´óÁ÷Á¿²ÉÑùÆ÷¾ÙÐвÉÑù£¬£¬£¬£¬£¬£¬£¬£¬GC-MS6800¼ì²âÇéÐÎ¿ÕÆøÖеÄÓлúÂÈũҩ£¬£¬£¬£¬£¬£¬£¬£¬ÒÇÆ÷ѸËٶȸߣ¬£¬£¬£¬£¬£¬£¬£¬ÎȹÌÐԺ㬣¬£¬£¬£¬£¬£¬£¬ÇÒÄܺܺõÄÖª×ã¹ú±êÒªÇ󡣡£¡£¡£¡£
4 ²Î¿¼±ê×¼
[1] HJ 900-2017 ÇéÐÎ¿ÕÆø
ÓлúÂÈũҩµÄ²â¶¨ ÆøÏàÉ«Æ×-ÖÊÆ×·¨