ÏÖ´úÅ©ÒµÉú²úÖÐÅ©Ò©µÄÆÕ±éÓ¦Ó㬣¬£¬£¬£¬£¬£¬£¬ÒѾ­³ÉΪ¿ÕÆøÎÛȾµÄÖ÷ҪȪԴ֮һ¡£¡£¡£¡£¡£¡£ÅçÈ÷ºóµÄÅ©Ò©¿ÉÒÔÂþÑÜÓÚ¿ÕÆø¡¢Ë®ºÍÍÁÈÀÖУ¬£¬£¬£¬£¬£¬£¬£¬¶øÖ±½ÓÊ©ÓÃÓÚÅ©×÷ÎïµÄÅ©Ò©Ôò»á»Ó·¢µ½¿ÕÆøÖС£¡£¡£¡£¡£¡£ÓлúÂÈÅ©Ò©×÷ΪÌìÏÂÉÏÉú²úºÍʹÓõÄÅ©Ò©Ö®Ò»£¬£¬£¬£¬£¬£¬£¬£¬Õý¾­ÓÉÖÖÖÖ;¾¶ÎÛȾ¿ÕÆø¡£¡£¡£¡£¡£¡£ÎªÁ˸üºÃµÄ¼ì²â¿ÕÆøÖкÛÁ¿ÓлúÂÈÅ©Ò©£¬£¬£¬£¬£¬£¬£¬£¬Ê¹ÓÃÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒǾßÓмì³öÏ޵ͣ¬£¬£¬£¬£¬£¬£¬£¬¶¨ÐÔÄÜÁ¦Ç¿¡¢¶¨Á¿×¼È·µÈÌص㣬£¬£¬£¬£¬£¬£¬£¬ÒÑÆÕ±éÓ¦ÓÃÓÚ¿ÕÆøÖкÛÁ¿Å©Ò©²ÐÁôµÄ¼ì²â¡£¡£¡£¡£¡£¡£

   luck18¹ÙÍøÒÇÆ÷Ò»Ö±ÖÂÁ¦ÓÚΪ¿Í»§Ìṩ¸üÍêÉƵĽâ¾ö¼Æ»®£¬£¬£¬£¬£¬£¬£¬£¬ÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇGC-MS 6800¿ÉÓÃÓÚÇéÐοÕÆøÖÐÓлúÂÈÅ©Ò©µÄ¼ì²â¡£¡£¡£¡£¡£¡£

   1.ÒÇÆ÷¼ò½é

GC-MS 6800ÊÇluck18¹ÙÍøÒÇÆ÷È«ÐÄ´òÔìµÄÒ»¿î¸ßÐÔ¼Û±ÈÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇ£¬£¬£¬£¬£¬£¬£¬£¬¾ßÓÐÍêÈ«µÄ×ÔÖ÷֪ʶ²úȨ£¬£¬£¬£¬£¬£¬£¬£¬ÓµÓжàÏîÊÖÒÕ£¬£¬£¬£¬£¬£¬£¬£¬¿ÉÆÕ±éÓ¦ÓÃÓÚÇéÐα£»£»£»£»£»£»¤¡¢µç×ÓµçÆ÷¡¢Ò½Ò©¡¢Ê¯ÓÍ»¯¹¤¡¢Ê³ÎïÇå¾²¡¢·Ä֯Ƥ¸ïµÈ¶àÐÐÒµÖÐÓк¦ÎïÖʵļì²â¡£¡£¡£¡£¡£¡£

ͼ1.  GC-MS 6800ÆøÏàÉ«Æ×-ÖÊÆ×ÁªÓÃÒÇÍâ¹Ûͼ

2 ʵÑ鲿·Ö

2.1 ²âÊÔÔ­Àí

ÓôóÁ÷Á¿²ÉÑùÆ÷½«ÇéÐοÕÆøÆøÏàºÍ¿ÅÁ£ÎïÖеÄÓлúÂÈÊÕÂÞµ½ÂËĤºÍ¾Û°±õ¥ÅÝÄ­£¨PUF£©ÉÏ£¬£¬£¬£¬£¬£¬£¬£¬ÓÃÒÒÃÑ-Õý¼ºÍé»ìÏýÈܼÁÌáÈ¡£¡£¡£¡£¡£¡£¬£¬£¬£¬£¬£¬£¬£¬ÌáÈ¡Òº¾­Å¨Ëõ¡¢¾»»¯ºó£¬£¬£¬£¬£¬£¬£¬£¬ÆøÏàÉ«Æ×ÊèÉ¢£¬£¬£¬£¬£¬£¬£¬£¬ÖÊÆ×ÒǼì²â£¬£¬£¬£¬£¬£¬£¬£¬Æ¾Ö¤±£´æʱ¼äºÍÌØÕ÷Àë×ÓƷò±È¶¨ÐÔ£¬£¬£¬£¬£¬£¬£¬£¬Äڱ귨¶¨Á¿¡£¡£¡£¡£¡£¡£

2.2 Ö÷ÒªÒÇÆ÷×°±¸¡¢ºÄ²ÄºÍÊÔ¼Á

GC-MS 6800 ÆøÏàÉ«Æ×-ÖÊÆ×ÁªÓÃÒÇ£¨luck18¹ÙÍø£©

´óÁ÷Á¿²ÉÑùÆ÷£¨600/AFPUF1001K Òâ´óÀû£©

Ë÷ʽÌáÈ¡ÒÇ£¨É½¶«º£ÄÜ£©

µª´µÒÇ£¨±±¾©ÓÅêÉÍŽá¿Æ¼¼ÓÐÏÞ¹«Ë¾£©

¹ÌÏàÝÍȡװÖã¨À³²®Ì©¿Æ£©

±ûͪ£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©

Õý¼ºÍ飨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©

ÒÒÃÑ£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©

¶þÂȼ×Í飨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©

ÎÞË®ÁòËáÄÆ£ºÆÊÎö´¿£¨½­ËÕÇ¿Ê¢¹¦Ð§»¯Ñ§ÓÐÏÞ¹«Ë¾£©

ÂÈ»¯ÄÆ£ºÆÊÎö´¿£¨½­ËÕÇ¿Ê¢¹¦Ð§»¯Ñ§ÓÐÏÞ¹«Ë¾£©

ÁòË᣺ÃܶÈ1.84g/cm³£¬£¬£¬£¬£¬£¬£¬£¬Óż¶´¿£¨HPLC¼¶£¬£¬£¬£¬£¬£¬£¬£¬Merck£©

ÂÈ»¯ÄÆÈÜÒº£º50g/L£¬£¬£¬£¬£¬£¬£¬£¬ÏÖÓÃÏÖÅä

ÄÚ±êʹÓÃÒº£ºÝì-d10,10ug/ml£¬£¬£¬£¬£¬£¬£¬£¬Õý¼ºÍéÉèÖã¨Öйú±ê×¼ÎïÖÊ£©

Ìæ»»ÎïʹÓÃÒº£ºÆp-d12£¬£¬£¬£¬£¬£¬£¬£¬2ug/ml£¨Öйú±ê×¼ÎïÖÊ£©

±ê×¼´¢±¸Òº£º10mg/L,ÈܼÁÕý¼ºÍ飨Öйú±ê×¼ÎïÖÊ£©

µªÆø£º´¿¶È¡Ý99.999%£¨¿ÕÆø»¯¹¤£©

º¤Æø£º´¿¶È¡Ý99.999%£¨¿ÕÆø»¯¹¤£©

2.3ÒÇÆ÷²âÊÔÌõ¼þ

É«Æ×Öù£ºDB-5MS£¬£¬£¬£¬£¬£¬£¬£¬30m¡Á0.25mm¡Á0.25¦Ìm£¨Agilent£©

ÖùÏä³ÌÐòÉýÎÂÌõ¼þ£º80¡æ£¨1min£©20¡æ/min 200¡æ 5¡æ/min 280¡æ£¨5min£©

½øÑù¿Úζȣº280¡æ£»£»£»£»£»£»ÆøÖʽӿÚζȣº280¡æ£»£»£»£»£»£»Àë×ÓԴζȣº280¡æ

ÔØÆø£ºº¤Æø£¬£¬£¬£¬£¬£¬£¬£¬´¿¶È¡Ý99.999%£¬£¬£¬£¬£¬£¬£¬£¬Á÷ËÙ1.0mL/min

µçÀë·½·¨£ºEI£»£»£»£»£»£»µçÀëÄÜÁ¿£º70eV

½øÑù·½·¨£º²»·ÖÁ÷½øÑù£¬£¬£¬£¬£¬£¬£¬£¬·ÖÁ÷±È20£º1£»£»£»£»£»£»½øÑùÁ¿£º1.0¦ÌL

²â¶¨·½·¨£ºTIC£¨FULL SCAN£©¶¨ÐÔ£¨É¨Ãè¹æÄ££º45-450amu£©£¬£¬£¬£¬£¬£¬£¬£¬SIMģʽ¶¨Á¿¡£¡£¡£¡£¡£¡£

 Í¼2. ÓлúÂÈÅ©Ò©»¯ºÏÎï×ÜÀë×ÓÁ÷É«Æ×ͼ

1¡ª¦Á-ÁùÁùÁù£»£»£»£»£»£»2¡ª¦Â-ÁùÁùÁù£»£»£»£»£»£»3¡ª¦Ã -ÁùÁùÁù£»£»£»£»£»£»4¡ªÝì-D10£¨Äڱ꣩£»£»£»£»£»£»5¡ª¦Ä-ÁùÁùÁù£»£»£»£»£»£»6¡ªÆßÂÈ£»£»£»£»£»£»7¡ª°¬ÊϼÁ£»£»£»£»£»£»8¡ª»·ÑõÆßÂÈ B£»£»£»£»£»£»9¡ª¦Ã-Âȵ¤£»£»£»£»£»£»£»£»£»£»£»£»10¡ªÁòµ¤ I£»£»£»£»£»£»11¡ª¦Á-Âȵ¤£»£»£»£»£»£»12¡ª4,4'-DDE£»£»£»£»£»£»13¡ªµÒÊϼÁ£»£»£»£»£»£» 14¡ªÒìµÒÊϼÁ£»£»£»£»£»£»15¡ªÁòµ¤ II£»£»£»£»£»£»16¡ª4,4'- DDD£»£»£»£»£»£» 17¡ªÒìµÒÊÏÈ©£»£»£»£»£»£»18¡ªÁòµ¤ÁòËáõ¥£»£»£»£»£»£»19¡ª 4,4'-DDT£»£»£»£»£»£»20¡ªÒìµÒÊÏͪ£»£»£»£»£»£» 21¡ª¼×Ñõ DDT£»£»£»£»£»£»22¡ªÆp-D12£¨²ÉÑùÌæ»»Î

3 С½á

    ½ÓÄÉ´óÁ÷Á¿²ÉÑùÆ÷¾ÙÐвÉÑù£¬£¬£¬£¬£¬£¬£¬£¬GC-MS6800¼ì²âÇéÐοÕÆøÖеÄÓлúÂÈÅ©Ò©£¬£¬£¬£¬£¬£¬£¬£¬ÒÇÆ÷ѸËٶȸߣ¬£¬£¬£¬£¬£¬£¬£¬ÎȹÌÐԺ㬣¬£¬£¬£¬£¬£¬£¬ÇÒÄܺܺõÄÖª×ã¹ú±êÒªÇ󡣡£¡£¡£¡£¡£

4 ²Î¿¼±ê×¼

[1] HJ 900-2017 ÇéÐοÕÆø ÓлúÂÈÅ©Ò©µÄ²â¶¨ ÆøÏàÉ«Æ×-ÖÊÆ×·¨